1-(3,4-二氢-6-甲基-2H-吡喃-2-基)-乙酮合成路线 （共 18 条）
反应条件
hydroquinone T=145°C; 24 h;
参考文献
Weyerstahl, Peter; Krohn, Kerstin
Tetrahedron, 1990 , vol. 46, # 10 p. 3503 - 3514
反应条件
magnesium oxide T=100°C; Robinson annelation; P=75007.5 Torr; 2 h;
参考文献
Kawanami, Hajime; Ikushima, Yutaka
Tetrahedron Letters, 2004 , vol. 45, # 26 p. 5147 - 5150
参考文献
Jun, Jong-Gab; Lee, In-Suk
Synthetic Communications, 2000 , vol. 30, # 7 p. 1159 - 1165
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Jun, Jong-Gab; Kim, Ae-Ran; Sung, Hoon Kim
Synthetic Communications, 2002 , vol. 32, # 1 p. 45 - 52
反应条件
1: With hydroquinone in benzene T=170°C; Diels-Alder reaction; 3 h; 2: With sodium hydroxide; water Hydrolysis; 12 h;
参考文献
Jun, Jong-Gab; Lee, In-Suk
Synthetic Communications, 2000 , vol. 30, # 7 p. 1159 - 1165
反应条件
1: With hydroquinone in benzene T=170°C; Diels-Alder reaction; 3 h; 2: With sodium hydroxide in water 12 h; 3: With hydrogenchloride in water
参考文献
Jun, Jong-Gab; Kim, Ae-Ran; Sung, Hoon Kim
Synthetic Communications, 2002 , vol. 32, # 1 p. 45 - 52
反应条件
1: With hydroquinone in benzene T=170°C; Diels-Alder reaction; 3 h; 2: With sodium hydroxide in water 12 h; 3: With bromine; sodium hydrogencarbonate in water T=20°C; 3 h;
参考文献
Jun, Jong-Gab; Kim, Ae-Ran; Sung, Hoon Kim
Synthetic Communications, 2002 , vol. 32, # 1 p. 45 - 52
反应条件
cadmium phosphate-calcium phosphate-catalyst; steam T=350 - 400°C;
参考文献
Gorin; Bogdanowa
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 657,660; engl. Ausg. S. 640, 642
反应条件
sodium carbonate 48 h; Heating; Title compound not separated from byproducts;
参考文献
Bridges, Alexander J.; Fischer, John W.
Journal of Organic Chemistry, 1984 , vol. 49, # 16 p. 2954 - 2961
反应条件
T=80°C; 8 h; Yield given. Title compound not separated from byproducts;
参考文献
Hopf, Henning; Jaeger, Helge; Ernst, Ludger
Liebigs Annales, 1996 , # 5 p. 815 - 824
反应条件
in ethylene glycol dimethyl ether; benzene Diels-Alder reaction; KineticsMechanism; Temperature;
参考文献
Wang, Zhihong; Hirschi, Jennifer S.; Singleton, Daniel A.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 48 p. 9156 - 9159
