PdCl(COPh)(PPh3)2 in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=65°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 48, # 24 p. 4634 - 4642
benzylchlorobis(triphenylphosphine)pa.. in chloroform T=65°C; other solvent; competition with Bu3SnPh; relative reaction rates of benzoyl chloride with organotins;
参考文献
Labadie,J.W.; Stille,J.K.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6129
1: N-methoxycarbonyl-2-trimethylsilylpyrrolidine With tetra-n-butylammonium tetrafluoroborate in dichloromethane T=-78°C; Electrolysis; 2: benzyltributylstannane in dichloromethane T=-50°C; 1.5 h; 3: With triethylamine in dichloromethane T=-50 - 20°C;
参考文献
Maruyama, Tomokazu; Mizuno, Yusuke; Shimizu, Ikuo; Suga, Seiji; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1902 - 1903
in benzene byproducts: bibenzyl; Irradiation (UV/VIS); 4.75 h irradn.; concg.; triturating with cold methanol; filtering; filtrate concg.; chromy. (alumina) eluting with CHCl3/petroleum; two fractions rechromy. (silica) with petroleum ether;
参考文献
Journal of the American Chemical Society, , vol. 103, # 24 p. 7235 - 7239
