4-硝基-1H-吡咯-2-甲酰氯合成路线 (共 2 条)
反应条件
thionyl chloride; triethylamine in ethylene glycol dimethyl ether T=0°C; 0.25 h;
参考文献
Cockroft, Scott L.; Perkins, Julie; Zonta, Cristiano; Adams, Harry; Spey, Sharon E.; Low, Caroline M. R.; Vinter, Jeremy G.; Lawson, Kevin R.; Urch, Christopher J.; Hunter, Christopher A.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 7 p. 1062 - 1080
反应条件
1: 100 percent / aq. KOH / 19 h / 100 °C 2: oxalyl chloride / CH2Cl2; dimethylformamide / 4.5 h / 20 °C View Scheme
参考文献
Lee; Coulter; Lown
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 1855 - 1859