ammonium chloride; hydroxocobalamine hydrochloride; zinc in water 6 h; Heatinginternal standard cyclohexanol, isomerization, different solvents (also deuterated ones), different reaction times; Product distribution;
ammonium chloride; hydroxocobalamine hydrochloride; zinc in water 6 h; Heatinginternal standard cyclohexanol, isomerization, different solvents (also deuterated ones), different reaction times; Product distribution;
1: With (R,R)-(-)-(salen)chromium chloride in acetonitrile T=20°C; 0.25 h; 2: With silver fluoride in acetonitrile T=50°C; 72 h; Further stages. Title compound not separated from byproducts.;
参考文献
Kalow, Julia A.; Doyle, Abigail G.
Journal of the American Chemical Society, 2011 , vol. 133, # 40 p. 16001 - 16012
