1H-苯并三唑-1-甲醇合成路线 （共 47 条）
参考文献
Gaylord; Naughton
Journal of Organic Chemistry, 1957 , vol. 22, p. 1022,1023
反应条件
1,4-dioxane; pyridine
参考文献
Gaylord; Naughton
Journal of Organic Chemistry, 1957 , vol. 22, p. 1022,1023
反应条件
in acetic acid
3 h; Heating;
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Synthesis, 1990 , p. 341 - 346
反应条件
in acetic acid
0.0666667 h; Heating;
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Synthesis, 1990 , p. 341 - 346
反应条件
1: SOCl2 / toluene / 2 h / Heating
2: 40 percent / methanol / 1 h / Heating
3: toluene; diethyl ether / Heating
View Scheme
参考文献
Katritzky, Alan R.; Rachwal, Stanislaw; Rachwal, Bogumila
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6022 - 6029
反应条件
1: With sodium sulfate in methanol
T=25°C; Mannich reaction; 10 h;
2: With aluminium trichloride in dichloromethane
10 h; Heating;
3: With sodium tetrahydroborate in tetrahydrofuran
T=25°C;
参考文献
Katritzky, Alan R; He, Hai-Ying; Jiang, Rong; Long, Qiuhe
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2427 - 2434
反应条件
1: 60 percent / acetic acid / 0.25 h / Heating
2: 70 percent / conc. HCl / methanol; H2O / 72 h / Heating
View Scheme
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Synthesis, 1990 , p. 341 - 346
参考文献
Gaylord
Journal of the American Chemical Society, 1954 , vol. 76, p. 285
参考文献
Gaylord; Naughton
Journal of Organic Chemistry, 1957 , vol. 22, p. 1022,1023
反应条件
1: 52 percent / HOAc / 48 h / Heating
2: 1.) nBuLi / 1.) THF, hexane, -78 deg C, 2 h, 2.) THF, room temperature, overnight
View Scheme
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Chemische Berichte, 1991 , vol. 124, # 8 p. 1819 - 1826
