1,4-二氧杂环庚烷-6-酮合成路线 (共 2 条)
反应条件
hydrogenchloride in water 2.5 h; Reflux;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH
Patent: US2012/196872 A1, 2012 ;
Location in patent: Page/Page column 38 ;
反应条件
1.1: sodium t-butanolate / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux 1.2: pH 5 / Inert atmosphere 2.1: hydrogenchloride / water / 2.5 h / Reflux View Scheme
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH
Patent: US2012/196872 A1, 2012 ;