4-乙酰氧基-2-氮杂环丁酮合成路线 (共 46 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
1) 0 deg C, 2 h, 2) RT, overnight;
参考文献
Pfaendler, Hans Rudolf; Hendel, Wolfram; Nagel, Ulrich
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1992 , vol. 47, # 7 p. 1037 - 1049
参考文献
Lee, Sang Hyup
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 121 - 127
反应条件
in benzene
24 h; Ambient temperature;
参考文献
Attrill; Barrett; Quayle; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1679 - 1682
反应条件
sodium tetrahydroborate in ethanol
1 h; Ambient temperature;
参考文献
Kametani, Tetsuji; Chu, Shih-Der; Itoh, Akira; Maeda, Sayuri; Honda, Toshio
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2683 - 2687
反应条件
1H-imidazole; sodium hydride
1.) THF, r.t., 2 h 2.) -78 deg C, 4h; Yield given. Multistep reaction;
参考文献
Attrill; Barrett; Quayle; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1679 - 1682
参考文献
Satoh, Hisao; Tsuji, Teruji
Tetrahedron Letters, 1984 , vol. 25, # 16 p. 1733 - 1736