in toluene dropwise addn. of Me2BBr in toluene to a stirred soln. of Si-compd. in toluene, briefly refluxed; solvent and Me3SiBr distd. off under reduced pressure, residue sublimed off (bath temp.: 110°C at 1E-3 Torr), sublimate recrystd. (heptane); elem. anal., sublimation residue contains oligomers: (Me2B(C2H2N3))(n);
参考文献
Niedenzu, K.; Woodrum, K. R.
Inorganic Chemistry, 1989 , vol. 28, p. 4022 - 4026
Gold; Sommer; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2874
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Gmelin Handbook: Si: MVol.C, 4, page 14 - 18