反应条件
1: (E)-ethanone-1-phenyl-O-(phenylmethyl)oxime With borane-THF; enantiopure spiroborate ester in tetrahydrofuran T=25°C; 36 h; 2: chloroformic acid ethyl ester With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=25°C; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Huang, Xiaogen; Ortiz-Marciales, Margarita; Huang, Kun; Stepanenko, Viatcheslav; Merced, Francisco G.; Ayala, Angel M.; Correa, Wildeliz; De Jesus, Melvin
Organic Letters, 2007 , vol. 9, # 9 p. 1793 - 1795
