2-Oxa双环[4.1.0]庚烷合成路线 （共 4 条）
反应条件
tetrabutylammomium bromide in dichloromethane; N,N-dimethyl-formamide T=40°C; electrolysis;
参考文献
Durandetti, Sylvie; Sibille, Soline; Perichon, Jacques
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3255 - 3258
反应条件
1: (E)-4-pentadien-1-ol With sodium hydride in tetrahydrofuran; mineral oil T=0°C; Inert atmosphere; 2: butyl 3-bromo-3H-diazirine-3-carboxylate in tetrahydrofuran; N,N-dimethyl-formamide; mineral oil T=-40 - 0°C; Inert atmosphere;
参考文献
Hanzlova, Eva; Navratil, Rafael; Cejka, Jan; Boehm, Stanislav; Martinuis, Tomas
Organic Letters, 2014 , vol. 16, # 3 p. 852 - 855
反应条件
Behandeln mit einer aus Dijodmethan und verkupfertem Zink in Aether hergestellten Loesung des Methylen-Zinkjodid-Assoziat;
参考文献
Shank; Shechter
Journal of Organic Chemistry, 1959 , vol. 24, p. 1825
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Simmons; Smith
Journal of the American Chemical Society, 1959 , vol. 81, p. 4256,4258, 4262
Org. Synth. Coll. Vol., 1973 , vol. V, p. 855
反应条件
[PtCl2(H2C=CH2)]2 in dichloromethane
20 h; Ambient temperature;
参考文献
Beyer; Skaanderup; Madsen
Journal of the American Chemical Society, 2000 , vol. 122, # 40 p. 9575 - 9583
