1,5:3,4-二去氢-2-脱氧戊糖醇合成路线 （共 3 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0 - 20°C; 19 h;
参考文献
ELI LILLY AND COMPANY; JADHAV, Prabhakar Kondaji; SAEED, Ashraf; GREEN, Jonathan Edward; KRISHNAN, Venkatesh; MATTHEWS, Donald Paul; STEPHENSON, Gregory Alan
Patent: WO2013/55577 A1, 2013 ;
Location in patent: Page/Page column 36-37 ;
反应条件
1: ethylene glycol; potassium hydroxide
2: chloroform; peroxybenzoic acid
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参考文献
Paul; Tchelitcheff
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1947 , vol. 224, p. 1722
反应条件
1.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C
1.2: 2 h / 50 - 100 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
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参考文献
XI, Ning; WANG, Tingjin; YI, Lei
Patent: WO2013/138210 A1, 2013 ;
