1,2-5,6-二环氧-环辛烷合成路线 (共 8 条)
反应条件
dihydrogen peroxide; tris(cetyl)pyridinium 12-tungstophosphate in water T=25°C; 17 h;
参考文献
Qiao, Yunxiang; Li, Huan; Hua, Li; Orzechowski, Lars; Yan, Kai; Feng, Bo; Pan, Zhenyan; Theyssen, Nils; Leitner, Walter; Hou, Zhenshan
ChemPlusChem, 2012 , vol. 77, # 12 p. 1128 - 1138
反应条件
dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water T=0 - 20°C;
参考文献
Akbulatov, Sergey; Tian, Yancong; Boulatov, Roman
Journal of the American Chemical Society, 2012 , vol. 134, # 18 p. 7620 - 7623
反应条件
2,2,2-Trifluoro-1-phenyl-ethanone; dihydrogen peroxide in acetonitrile; tert-butyl alcohol T=20°C; 1 h; Green chemistry;
参考文献
Limnios, Dimitris; Kokotos, Christoforos G.
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4270 - 4276
反应条件
phosphoric acid; sulfuric acid; dihydrogen peroxide; sodium tungstate; Aliquatreg; 336 in water; 1,2-dichloro-ethane T=70°C; pH=1.6; 1 h; microwave irradiation;
参考文献
Bogdal; Lukasiewicz; Pielichowski; Bednarz
Synthetic Communications, 2005 , vol. 35, # 23 p. 2973 - 2983
反应条件
sodium hydroxide in chloroform; water
参考文献
Ciba-Geigy Corporation
Patent: US4412047 A1, 1983 ;
反应条件
oxygen; isobutyraldehyde in acetonitrile T=60°C; 4 h;
参考文献
Pielichowski, Jan; Kowalski, Grzegorz
Molecular Crystals and Liquid Crystals, 2010 , vol. 522, p. 105 - 111
反应条件
oxygen T=90°C; 3.5 h; var. reaction procedures, also in the presence of initiator and inhibitor of free-radical reaction; Product distributionMechanism;
参考文献
Giezynski, Roman; Pala, Magdalena
Polish Journal of Chemistry, 1986 , vol. 60, # 1-3 p. 85 - 90
反应条件
ammonia; iodine in water; acetonitrile T=70°C;
参考文献
Chemistry Letters, , vol. 42, # 2 p. 162 - 164