(2,4,6-环庚三烯-1-亚基)丙二腈合成路线 (共 12 条)
反应条件
in chlorobenzene T=130°C; 20 h; study of the cycloaddition reaction, in sealed tube at elevated temperature, mechanism of the <4+2>adduct formation is discussed; Product distributionMechanism;
参考文献
Tian, Guan Rong; Sugiyama, Shigeru; Mori, Akira; Takeshita, Hitoshi; Higashi, Miwako; Yamaguchi, Hiroyuki
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1136 - 1142
反应条件
pyridine
T=0 - 40°C; 6.16667 h; Inert atmosphere;
参考文献
Yang, Xianghua; Fox, Thomas; Berke, Heinz
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 852 - 860
反应条件
in chloroform
168 h; Ambient temperature;
参考文献
Liu, Ching-Yang; Ding, Shuenn-Tarng
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4539 - 4544
反应条件
T=450°C; P=0.0001 Torr; 10 h;
参考文献
Hoffmann, Reinhard W.; Riemann, Achim; Mayer, Bernhard
Chemische Berichte, 1985 , vol. 118, # 6 p. 2493 - 2513
反应条件
oxygen in hexane
0.25 h; Irradiation; Further byproducts given;
参考文献
Hirano, Takashi; Kumagai, Tsutomu; Miyashi, Tsutomu; Akiyama, Kimio; Ikegami, Yusaku
Journal of Organic Chemistry, 1992 , vol. 57, # 3 p. 876 - 882
反应条件
benzophenone in benzene
11 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Hirano, Takashi; Kumagai, Tsutomu; Miyashi, Tsutomu; Akiyama, Kimio; Ikegami, Yusaku
Journal of Organic Chemistry, 1992 , vol. 57, # 3 p. 876 - 882
反应条件
furan; benzophenone in benzene
11 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Hirano, Takashi; Kumagai, Tsutomu; Miyashi, Tsutomu; Akiyama, Kimio; Ikegami, Yusaku
Journal of Organic Chemistry, 1992 , vol. 57, # 3 p. 876 - 882
反应条件
T=140 - 150°C; P=0.01 Torr;
参考文献
Haug,E.; Foehlisch,B.
Chemische Berichte, 1971 , vol. 104, p. 2670 - 2680
反应条件
acetic anhydride; triethylamine in dichloromethane
参考文献
Jutz,C.
Chemische Berichte, 1964 , vol. 97, p. 2050 - 2065
反应条件
benzophenone
3 h; Irradiationmolecular sieve (4A); Further byproducts given;
参考文献
Hirano, Takashi; Kumagai, Tsutomu; Miyashi, Tsutomu; Akiyama, Kimio; Ikegami, Yusaku
Journal of Organic Chemistry, 1992 , vol. 57, # 3 p. 876 - 882