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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-二甲基氨基苯硼酸
合成路线
（共 34 条）
28611-39-4
4-二甲基氨基苯硼酸
+
586-78-7
1-溴-4-硝基苯
→
反应条件
2143-87-5
4-二甲氨基-4'-硝基联苯
反应条件
potassium carbonate in ethanol; water T=80°C; Suzuki coupling; 0.166667 h; Microwave irradiation;
参考文献
Siamaki, Ali R.; Khder, Abd El Rahman S.; Abdelsayed, Victor; El-Shall, M. Samy; Gupton, B. Frank
Journal of Catalysis, 2011 , vol. 279, # 1 p. 1 - 11
28611-39-4
4-二甲基氨基苯硼酸
+
100-63-0
苯肼
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
591-50-4
碘苯
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
反应条件
stilbazo; palladium diacetate; potassium carbonate in water T=20°C; Suzuki-Miyaura cross-coupling reaction; Inert atmosphere;
参考文献
Peng, Yi-Yuan; Liu, Jinbiao; Lei, Xiaoli; Yin, Zenlan
Green Chemistry, 2010 , vol. 12, # 6 p. 1072 - 1075
108-86-1
溴代苯
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
反应条件
stilbazo; palladium diacetate; potassium carbonate in water T=20°C; Suzuki-Miyaura cross-coupling reaction; Inert atmosphere;
参考文献
Peng, Yi-Yuan; Liu, Jinbiao; Lei, Xiaoli; Yin, Zenlan
Green Chemistry, 2010 , vol. 12, # 6 p. 1072 - 1075
2516-40-7
2-溴苯并噻唑
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
10205-56-8
(4-苯并噻唑-2-基-苯基)-二甲基-胺
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether; water T=150°C; Suzuki coupling; Microwave irradiationCombinatorial reaction / High throughput screening (HTS);
参考文献
Auld, Douglas S.; Zhang, Ya-Qin; Southall, Noel T.; Rai, Ganesha; Landsman, Marc; MacLure, Jennifer; Langevin, Daniel; Thomas, Craig J.; Austin, Christopher P.; Inglese, James
Journal of Medicinal Chemistry, 2009 , vol. 52, # 5 p. 1450 - 1458
623-03-0
对氯苯甲腈
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
27104-69-4
4-联苯甲腈
反应条件
4,4'-(phenylphosphinediyl)bis(2,6-dimethylmorpholine); caesium carbonate; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane Suzuki-Miyaura coupling; 6 h; Heating;
参考文献
Cho, Su-Dong; Kim, Ho-Kyun; Yim, Heung-seop; Kim, Mi-Ra; Lee, Jin-Kook; Kim, Jeum-Jong; Yoon, Yong-Jin
Tetrahedron, 2007 , vol. 63, # 6 p. 1345 - 1352
→
反应条件
27104-69-4
4-联苯甲腈
反应条件
potassium carbonate in ethanol; water T=20°C; Suzuki Coupling; 0.5 h; Microwave irradiationSealed tube;
参考文献
Siamaki, Ali R.; Lin, Yi; Woodberry, Kendra; Connell, John W.; Gupton, B. Frank
Journal of Materials Chemistry A, 2013 , vol. 1, # 41 p. 12909 - 12918
91-22-5
喹啉
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
16032-41-0
反应条件
1: 4-(N,N-dimethylamino)phenylboronic acid With diethylzinc in 1,4-dioxane T=60°C; 12 h; 2: quinoline With [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine in 1,4-dioxane; toluene T=130°C; 20 h;
参考文献
Hyodo, Isao; Tobisu, Mamoru; Chatani, Naoto
Chemistry - An Asian Journal, 2012 , vol. 7, # 6 p. 1357 - 1365
29421-73-6
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
813450-64-5
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran; water Suzuki coupling; Inert atmosphereReflux;
参考文献
Ordronneau, Lucie; Nitadori, Hiroyuki; Ledoux, Isabelle; Singh, Anu; Williams, J. A. Gareth; Akita, Munetaka; Guerchais, Veronique; Le Bozec, Hubert
Inorganic Chemistry, 2012 , vol. 51, # 10 p. 5627 - 5636
541-59-3
马来酰亚胺
+
28611-39-4
4-二甲基氨基苯硼酸
→
反应条件
69006-87-7
反应条件
potassium hydroxide; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,4-dioxane; water T=100°C; 0.0833333 h; microwave irradiation;
参考文献
Iyer, Pravin S.; O'Malley, Meaghan M.; Lucas, Matthew C.
Tetrahedron Letters, 2007 , vol. 48, # 25 p. 4413 - 4418
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