6-硝基-2-苯并噻唑啉酮合成路线 (共 14 条)
反应条件
1: PCl5; POCl3 2: tin; aqueous HCl; acetic acid View Scheme
参考文献
Yakugaku Zasshi, , vol. 62, p. 47,51; dtsch. Ref. S. 19, 22
Chem.Abstr., , p. 609
反应条件
phosphorus pentachloride; trichlorophosphate
参考文献
Yakugaku Zasshi, , vol. 62, p. 47,51; dtsch. Ref. S. 19, 22
Chem.Abstr., , p. 609
反应条件
1: K2CO3 / ethanol / Heating 2: Fe, aq. HCl / ethanol 3: 3 h / 90 - 100 °C 4: (i) biphenyl, diphenyl ether, (ii) /BRN= 505934/, K2CO3, DMF 5: aq. HCl, AcOH / Heating View Scheme
参考文献
Suzuki; Kadoya; Dohmori
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 5 p. 1050 - 1058
反应条件
potassium hydroxide in water 1.) 90 deg C - 100 deg C, 24 h; 2.) 25 deg C - 30 deg C, 18 h.;
参考文献
D'Amico, John J.; Bollinger, Frederic G.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1601 - 1605