2,4-二苯基-5(4H)-噁唑酮合成路线 (共 20 条)
反应条件
in toluene T=110°C; 3 h; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 17 p. 2499 - 2502
反应条件
in water
T=25°C; 20 h; biosynthesis by lipase from Aspergillus niger (AP); phosphate buffer, pH: 7.6; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gu, Rui-Lin; Lee, Ik-Soo; Sih, Charles J.
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 1953 - 1956
反应条件
sodium carbonate; tetrabutylammomium bromide in dichloromethane; water
0.166667 h; Ambient temperature;
参考文献
Gelmi; Pocar; Rossi
Synthesis, 1984 , vol. NO. 9, p. 763 - 765
反应条件
palladium diacetate; (1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; potassium carbonate in toluene
T=80°C; 14 h;
参考文献
Liu, Xiaoxiang; Hartwig, John F
Organic letters, 2003 , vol. 5, # 11 p. 1915 - 1918
反应条件
18-crown-6 ether in benzene
24 h;
参考文献
Muneer, Mohammed; Tikare, Ravindra K.; Kamat, Prashant V.; George, Manapurathu V.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1624 - 1630
反应条件
potassium in tetrahydrofuran
4 h;
参考文献
Muneer, Mohammed; Tikare, Ravindra K.; Kamat, Prashant V.; George, Manapurathu V.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1624 - 1630
反应条件
polymer supported rose bengal; oxygen in N,N-dimethyl-formamide
Irradiation; Mechanism;
参考文献
Kato, Hiroshi; Tani, Kazue; Kurumisawa, Haruki; Tamura, Yoshiko
Chemistry Letters, 1980 , p. 717 - 720
反应条件
in toluene
T=110°C; 3 h; Further byproducts given;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; Rosa, Concetta La
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2499 - 2502
反应条件
in toluene
T=110°C; 3 h; Product distributionMechanism;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; Rosa, Concetta La
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2499 - 2502
反应条件
1: xylene / 0.33 h / 80 °C
2: 20percent NaOH / methanol / 0.5 h / Heating
View Scheme
参考文献
Rodriguez, H.; Pavez, H.; Marquez, A.; Navarrete, P.
Tetrahedron, 1983 , vol. 39, # 1 p. 23 - 27