2,2'-(1,4-亚苯基)二(1H-苯并咪唑-5-胺)合成路线 （共 6 条）
反应条件
acetic acid; zinc T=0°C; 3 h;
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
反应条件
1: 72 percent / hydrogen / Raney-nickel / ethanol / 8 h / 2660 Torr 2: 58 percent / conc. HCl / ethanol / 10 h / Heating 3: 75 percent / H2SO4, nitric acid / 1 h / 0 °C 4: 73 percent / zinc dust, acetic acid / 3 h / 0 °C View Scheme
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
反应条件
1: 75 percent / TEA / benzene / 14 h / Ambient temperature 2: 72 percent / hydrogen / Raney-nickel / ethanol / 8 h / 2660 Torr 3: 58 percent / conc. HCl / ethanol / 10 h / Heating 4: 75 percent / H2SO4, nitric acid / 1 h / 0 °C 5: 73 percent / zinc dust, acetic acid / 3 h / 0 °C View Scheme
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
反应条件
1: 75 percent / TEA / benzene / 14 h / Ambient temperature 2: 72 percent / hydrogen / Raney-nickel / ethanol / 8 h / 2660 Torr 3: 58 percent / conc. HCl / ethanol / 10 h / Heating 4: 75 percent / H2SO4, nitric acid / 1 h / 0 °C 5: 73 percent / zinc dust, acetic acid / 3 h / 0 °C View Scheme
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
反应条件
1: 58 percent / conc. HCl / ethanol / 10 h / Heating 2: 75 percent / H2SO4, nitric acid / 1 h / 0 °C 3: 73 percent / zinc dust, acetic acid / 3 h / 0 °C View Scheme
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
反应条件
1: 75 percent / H2SO4, nitric acid / 1 h / 0 °C 2: 73 percent / zinc dust, acetic acid / 3 h / 0 °C View Scheme
参考文献
Chauhan, P. M. S.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1146 - 1149
