1: With hydrogenchloride; sodium nitrite in water T=0°C; Diazotization; 0.166667 h; 2: With potassium iodide in water Iodination; 0.5 h;
参考文献
Bowden, Roy D.; Comina, Paul J.; Greenhall, Martin P.; Kariuki, Benson M.; Loveday, Amanda; Philp, Douglas
Tetrahedron, 2000 , vol. 56, # 21 p. 3399 - 3408
1.1: 48 percent / H2 / Pd/C / ethanol 2.1: NaNO2; conc. HCl / H2O / 0.17 h / 0 °C 2.2: 50 percent / KI / H2O / 0.5 h View Scheme
参考文献
Bowden, Roy D.; Comina, Paul J.; Greenhall, Martin P.; Kariuki, Benson M.; Loveday, Amanda; Philp, Douglas
Tetrahedron, 2000 , vol. 56, # 21 p. 3399 - 3408
→
反应条件
sodium iodide in acetonitrile
参考文献
Okazaki, Takao; Laali, Kenneth K.; Bunge, Scott D.; Adas, Sonya K.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1630 - 1644
