7-(二乙胺基)香豆素-3-甲酸乙酯合成路线 （共 8 条）
反应条件
piperidine in acetonitrile Knoevenagel condensation; 3 h; Heating;
参考文献
Muller, Caroline; Even, Pascale; Viriot, Marie-Laure; Carre, Marie-Christiane
Helvetica Chimica Acta, 2001 , vol. 84, # 12 p. 3735 - 3741
反应条件
anhydrous iron chloride in ethanol T=80°C; 24 h; Mechanism;
参考文献
He, Xinwei; Yan, Zhenglei; Hu, Xiaoqian; Zuo, Yin; Jiang, Chang; Jin, Lei; Shang, Yongjia
Synthetic Communications, 2014 , vol. 44, # 10 p. 1507 - 1514
反应条件
titanium tetrachloride in tetrahydrofuran Heating;
参考文献
Bissell
Synthesis, 1982 , vol. No. 10, p. 846 - 848
反应条件
sodium hydroxide in methanol
参考文献
Wells, Geoffrey; Suggitt, Marie; Coffils, Marissa; Baig, Mirza A.H.; Howard, Philip W.; Loadman, Paul M.; Hartley, John A.; Jenkins, Terence C.; Thurston, David E.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 6 p. 2147 - 2151
反应条件
hydrazine hydrate in ethanol T=20°C; 0.2 h;
参考文献
Xing, Zhitao; Wang, Hui-Chen; Cheng, Yixiang; James, Tony D.; Zhu, Chengjian
Chemistry - An Asian Journal, 2011 , vol. 6, # 11 p. 3054 - 3058
反应条件
hydrogenchloride 10 h; Heating;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 4 p. 888 - 892,793 - 796
反应条件
1: hydrogenchloride / water / 100 °C
2: trichlorophosphate / 60 °C
View Scheme
参考文献
Sanap, Kailas K.; Samant, Shriniwas D.
Synlett, 2012 , vol. 23, # 15 p. 2189 - 2194
反应条件
1: 87 percent / conc. aq. HCl / 10 h / Heating
2: 67 percent / POCl3 / 3 h / 80 °C
View Scheme
参考文献
An, Kyoung Lyong; Shin, Seung Rim; Jun, Kun; Park, Soo Youl
Journal of the Korean Chemical Society, 2014 , vol. 58, # 3 p. 297 - 302
