5,6,7,8-四氢-3-甲基喹啉合成路线 （共 52 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
5 h; Ambient temperature;
参考文献
Lippe, Gotelind von der; Weber, Horst
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 12 p. 1723 - 1726
反应条件
1: 22 g / acetic anhydride / 30 h / Heating
2: 22 g / hydrogen / 10percent palladium on carbon / ethanol / 1.5 h / 25 °C / 760 Torr
3: 1.) butyl-lithium / 1.) THF, hexane, 0.5 h, below 10 deg C 2.) 0.5 h, THF, hexane
View Scheme
参考文献
Crossley, Roger; Shepherd, Robin G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1917 - 1920
反应条件
1: 91 percent / 3-chloroperbenzoic acid / CHCl3 / 5 h / Ambient temperature
2: 1.) Ac2O, 2.) 10percent NaOH / 1.) 90 - 110 deg C, 15 h; 2.) reflux, 3 h
View Scheme
参考文献
John Wyeth and Brother Limited
Patent: US4011229 A1, 1977 ;
反应条件
hydrogenchloride; n-butyllithium; CO2 in methanol; hexane; water
参考文献
John Wyeth and Brother Limited
Patent: US4029668 A1, 1977 ;
反应条件
phenyllithium in CO2; water
参考文献
John Wyeth and Brother Limited
Patent: US4029668 A1, 1977 ;
反应条件
n-butyllithium in hexane
参考文献
John Wyeth and Brother Limited
Patent: US4000142 A1, 1976 ;
反应条件
n-butyllithium in hexane
参考文献
John Wyeth and Brother Ltd.
Patent: US4085108 A1, 1978 ;
反应条件
n-butyllithium in hexane; water; benzene
参考文献
John Wyeth and Brother Limited
Patent: US4000142 A1, 1976 ;
反应条件
n-butyllithium in water; benzene
参考文献
John Wyeth and Brother Limited
Patent: US4000142 A1, 1976 ;
反应条件
n-butyllithium in hexane; water; benzene
参考文献
John Wyeth and Brother Ltd.
Patent: US4085108 A1, 1978 ;
