三-O-乙酰基-D- 葡萄烯糖合成路线 （共 170 条）
反应条件
1: With hydrogen bromide; acetic anhydride T=20°C; 2: With sodium acetate; copper(II) sulfate; acetic acid; zinc in water 3.5 h; Further stages.;
参考文献
Banaag, April R.; Tius, Marcus A.
Journal of the American Chemical Society, 2007 , vol. 129, # 17 p. 5328 - 5329
反应条件
β-cyclodextrin; zinc in water T=20°C; 0.5 h; Sonication;
参考文献
Zhao, Jinzhong; Shao, Huawu; Wu, Xin; Shi, Shaojing
Chinese Journal of Chemistry, 2011 , vol. 29, # 7 p. 1434 - 1440
反应条件
indium(III) chloride; indium; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=20°C; 8 h;
参考文献
Cho, Sangwon; Kang, Soyeon; Keum, Gyochang; Kang, Soon Bang; Han, So-Yeop; Kim, Youseung
Journal of Organic Chemistry, 2003 , vol. 68, # 1 p. 180 - 182
反应条件
anhydrous iron chloride; para-fluorostyrene in tetrahydrofuran T=0 - 20°C; 1 h; diastereoselective reaction;
参考文献
Nicolas, Lionel; Angibaud, Patrick; Stansfield, Ian; Bonnet, Pascal; Meerpoel, Lieven; Reymond, Sebastien; Cossy, Janine
Angewandte Chemie - International Edition, 2012 , vol. 51, # 44 p. 11101 - 11104
Angew. Chem., 2012 , vol. 124, # 44 p. 11263 - 11266,4
反应条件
1.1: red phosphorus; Br2 / acetic anhydride / 25 °C 1.2: H2O / 13 h / 30 °C 2.1: 1.36 kg / NaOAc; CuSO4*5H2O; Zn / acetic acid; H2O / 50 °C View Scheme
参考文献
Apicore, LLC
Patent: US2013/5954 A1, 2013 ;
Location in patent: Page/Page column 15 ;
反应条件
1: With hydrogen bromide; acetic acid T=20°C; 2: With CuSO4‵5H2O; water; sodium acetate; zinc T=20°C; 1.5 h;
参考文献
Freitas, Juliano C.R.; Couto, Tulio R.; Paulino, Antonio A.S.; De Freitas Filho, Joao R.; Malvestiti, Ivani; Oliveira, Roberta A.; Menezes, Paulo H.
Tetrahedron, 2012 , vol. 68, # 41 p. 8645 - 8654
反应条件
anhydrous iron chloride; jackiePhos in tetrahydrofuran T=20°C; 1 h; Reagent/catalystSolventTemperature; diastereoselective reaction;
参考文献
Nicolas, Lionel; Angibaud, Patrick; Stansfield, Ian; Bonnet, Pascal; Meerpoel, Lieven; Reymond, Sebastien; Cossy, Janine
Angewandte Chemie - International Edition, 2012 , vol. 51, # 44 p. 11101 - 11104
Angew. Chem., 2012 , vol. 124, # 44 p. 11263 - 11266,4
反应条件
1: With hydrogen bromide in acetic acid T=0 - 20°C; Inert atmosphere; 2: With sodium acetate; acetic acid; zinc in dichloromethane; water T=0°C;
参考文献
Chao, Chin-Sheng; Lin, Ching-Yu; Mulani, Shaheen; Hung, Wei-Cheng; Mong, Kwok-Kong Tony
Chemistry - A European Journal, 2011 , vol. 17, # 43 p. 12193 - 12202
反应条件
Ni(COD)2; Pybox in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
Ag(1+)*C14H24AgN4O2(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
