三-O-乙酰基-D- 葡萄烯糖合成路线 （共 170 条）
反应条件
didodecanoyl peroxide in 1,2-dichloro-ethane Heating;
参考文献
Ouvry, Gilles; Quiclet-Sire, Beatrice; Zard, Samir Z.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 30 p. 5002 - 5006
反应条件
Ni(COD)2; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
Ni(COD)2; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
Ni(COD)2; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
Ni(COD)2; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
ethylene glycol dimethyl ether; nickel dichloride; Pybox in 1,3-dimethyl-imidazolidin-2-one; ethylene glycol dimethyl ether T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
1: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: MeZnI 12 h; Title compound not separated from byproducts;
参考文献
Gong, Hegui; Sinisi, Riccardo; Gagne, Michel R.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1908 - 1909
反应条件
1-methyl-1H-imidazole; zinc in ethyl acetate 18 h; RefluxInert atmosphere;
参考文献
Wolf, Saskia; Berrio, Rosmirt Molina; Meier, Chris
European Journal of Organic Chemistry, 2011 , # 31 p. 6304 - 6313
反应条件
[Cp2Ti(III)Cl]2 in tetrahydrofuran Ambient temperature;
参考文献
Spencer, Roxanne P.; Schwartz, Jeffrey
Tetrahedron Letters, 1996 , vol. 37, # 25 p. 4357 - 4360
反应条件
1: 2,3,4,6-Tetra-O-acetyl-α-D-mannopyranosyl bromide With N,N-dimethylimidazolone; ethylene glycol dimethyl ether; nickel dichloride T=20°C; 0.333333 h; 2: bromo(4-ethoxy-4-oxobutyl)zinc 12 h; Title compound not separated from byproducts;
参考文献
Gong, Hegui; Sinisi, Riccardo; Gagne, Michel R.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1908 - 1909
