三-O-乙酰基-D- 葡萄烯糖合成路线 (共 170 条)
反应条件
[Cp2Ti(III)Cl]2 in tetrahydrofuran Ambient temperatureother glycosyl halides, other unsaturated organic compounds; Mechanism;
参考文献
Spencer, Roxanne P.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4204 - 4205
反应条件
samarium diiodide in tetrahydrofuran Ambient temperatureslow addition of SmI2; Yield given;
参考文献
Doisneau, Gilles; Beau, Jean-Marie
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3477 - 3480
反应条件
N(Et)4ClO4 in acetonitrile T=20°C; Electrochemical reaction;
参考文献
Guerrini, Marco; Guglieri, Sara; Santarsiero, Roberto; Vismara, Elena
Tetrahedron Asymmetry, 2005 , vol. 16, # 1 p. 243 - 253
反应条件
1: 93 percent Spectr. / TMS-Br / CH2Cl2 2: 95 percent / (Cp2TiCl)2 / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cavallaro, Cullen L.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 7055 - 7057
反应条件
in benzene T=24°C; 144 h;
参考文献
Kudelska, Wieslawa; Michalska, Maria
Tetrahedron, 1981 , vol. 37, # 17 p. 2989 - 2994
反应条件
sodium acetate; copper(II) sulfate; acetic acid; zinc 20 h;
参考文献
Blattner, Regine; Ferrier, Robert J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1523 - 1527
反应条件
1: pyridine / 18 h / 20 °C / Inert atmosphere 2: hydrogen bromide / dichloromethane / 96 h / 20 °C / Inert atmosphere 3: 1-methyl-1H-imidazole; zinc / ethyl acetate / 18 h / Reflux; Inert atmosphere View Scheme
参考文献
Wolf, Saskia; Berrio, Rosmirt Molina; Meier, Chris
European Journal of Organic Chemistry, 2011 , # 31 p. 6304 - 6313
反应条件
1: hydrogen bromide / dichloromethane / 96 h / 20 °C / Inert atmosphere 2: 1-methyl-1H-imidazole; zinc / ethyl acetate / 18 h / Reflux; Inert atmosphere View Scheme
参考文献
Wolf, Saskia; Berrio, Rosmirt Molina; Meier, Chris
European Journal of Organic Chemistry, 2011 , # 31 p. 6304 - 6313
反应条件
pyridine; copper(l) iodide; methyllithium in diethyl ether a) -20 deg C, 1 h, b) 0 deg C, 2 h;
参考文献
Bellosta; Czernecki
Carbohydrate Research, 1993 , vol. 244, # 2 p. 275 - 284
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran Ambient temperature;
参考文献
Doisneau, Gilles; Beau, Jean-Marie
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3477 - 3480