1,4,5,6-四氢-3-苯基环戊并吡唑合成路线 （共 12 条）
反应条件
sodium acetate; acetic acid 3 h; Heating;
参考文献
Hussein; Sherif; Atalla
Monatshefte fur Chemie, 1996 , vol. 127, # 11 p. 1153 - 1160
反应条件
hydrazine hydrate in acetic acid T=20°C; 3 h;
参考文献
Atobe, Masakazu; Naganuma, Kenji; Kawanishi, Masashi; Morimoto, Akifumi; Kasahara, Ken-Ichi; Ohashi, Shigeki; Suzuki, Hiroko; Hayashi, Takahiko; Miyoshi, Shiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 5 p. 1327 - 1333
反应条件
in benzene 0.75 h; Heating;
参考文献
Padwa, Albert; Eisenbarth, Philipp
Tetrahedron, 1985 , vol. 41, # 2 p. 283 - 296
反应条件
in benzene 85 deg C 20 min then cooling to r.t.;
参考文献
Padwa, Albert; Eisenbarth, Philipp
Tetrahedron, 1985 , vol. 41, # 2 p. 283 - 296
反应条件
1: 85 percent / piperidine / ethanol / 3 h / Heating 2: 82 percent / NaOAc / acetic acid / 3 h / Heating View Scheme
参考文献
Atobe, Masakazu; Naganuma, Kenji; Kawanishi, Masashi; Morimoto, Akifumi; Kasahara, Ken-Ichi; Ohashi, Shigeki; Suzuki, Hiroko; Hayashi, Takahiko; Miyoshi, Shiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 5 p. 1327 - 1333
反应条件
1: diethyl ether View Scheme
参考文献
Eistert,B.; Wurzler,H.
Justus Liebigs Annalen der Chemie, 1961 , vol. 650, p. 157 - 170
反应条件
semicarbazide-hydrochloride in methanol; water Heating;
参考文献
Eistert,B.; Wurzler,H.
Justus Liebigs Annalen der Chemie, 1961 , vol. 650, p. 157 - 170
反应条件
1: lithium hexamethyldisilazane / toluene / 1 h / 0 °C 2: hydrazine hydrate / acetic acid / 3 h / 20 °C View Scheme
参考文献
Atobe, Masakazu; Naganuma, Kenji; Kawanishi, Masashi; Morimoto, Akifumi; Kasahara, Ken-Ichi; Ohashi, Shigeki; Suzuki, Hiroko; Hayashi, Takahiko; Miyoshi, Shiro
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 5 p. 1327 - 1333
反应条件
1: 50 percent / benzene / 0.5 h / Ambient temperature 2: 82 percent / benzene / 0.75 h / Heating View Scheme
参考文献
Padwa, Albert; Eisenbarth, Philipp
Tetrahedron, 1985 , vol. 41, # 2 p. 283 - 296
反应条件
1: 50 percent / benzene / 0.5 h / Ambient temperature 2: 82 percent / benzene / 0.75 h / Heating View Scheme
参考文献
Padwa, Albert; Eisenbarth, Philipp
Tetrahedron, 1985 , vol. 41, # 2 p. 283 - 296
