氯化-1-(苯甲基)吡啶翁合成路线 （共 22 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=52°C; P=736 Torr; 3 h;
参考文献
Paglietti, Giuseppe; Sanna, Paolo; Nuvole, Antonio; Soccolini, Francesco; Acheson, R. Morrin
Journal of Chemical Research, Miniprint, 1983 , # 10 p. 2326 - 2342
反应条件
0.333333 h; Heating;
参考文献
Tolstikova; Shainyan
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 7 p. 1068 - 1074
反应条件
1: 89 percent / 20 h / 100 °C
2: 66 percent / Na2S2O4, Na2CO3 / H2O / 1 h / 50 °C
3: 37 percent / H2 / 10percent Pd/C / ethanol / 3 h / 52 °C / 736 Torr
View Scheme
参考文献
Paglietti, Giuseppe; Sanna, Paolo; Nuvole, Antonio; Soccolini, Francesco; Acheson, R. Morrin
Journal of Chemical Research, Miniprint, 1983 , # 10 p. 2326 - 2342
反应条件
1: 89 percent / 20 h / 100 °C
2: 66 percent / Na2S2O4, Na2CO3 / H2O / 1 h / 50 °C
3: 37 percent / H2 / 10percent Pd/C / ethanol / 3 h / 52 °C / 736 Torr
View Scheme
参考文献
Paglietti, Giuseppe; Sanna, Paolo; Nuvole, Antonio; Soccolini, Francesco; Acheson, R. Morrin
Journal of Chemical Research, Miniprint, 1983 , # 10 p. 2326 - 2342
反应条件
p-toluenesulfonyl chloride
参考文献
Ferns; Lapworth
Journal of the Chemical Society, 1912 , vol. 101, p. 284
反应条件
in acetonitrile
40 h; Heating;
参考文献
Hale, P. D.; Boguslavsky, L. I.; Skotheim, T. A.; Karan, H. I.; Lan, H. L.; Okamoto, Y.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 190, p. 259 - 264
参考文献
v. Walther; Weinhagen
Journal fuer Praktische Chemie (Leipzig), 1917 , vol. <2> 96, p. 54
反应条件
potassium hydroxide; water; potassium hexacyanoferrate(III)
参考文献
Hamer; Kelly
Journal of the Chemical Society, 1931 , p. 777,781
反应条件
1.1: sodium tetrahydroborate / ethanol / 20 h / 0 - 20 °C
2.1: trifluoroacetic acid / dichloromethane / 0 - 5 °C
2.2: 0.42 h / 0 - 6 °C
2.3: -15 - 10 °C
View Scheme
参考文献
Scheunemann, Matthias; Hennig, Lothar; Funke, Uta; Steinbach, Joerg
Tetrahedron, 2011 , vol. 67, # 19 p. 3448 - 3456
反应条件
sodium tetrahydroborate
参考文献
Banwell, Martin G.; Coster, Mark J.; Harvey, Michael J.; Moraes, John
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 613 - 616
