5-溴-4-甲基-2-苯基-1,3-噻唑合成路线 （共 7 条）
反应条件
bromine in carbon disulfide Ambient temperature;
参考文献
Uchida, Kingo; Ishikawa, Takayuki; Takeshita, Michinori; Irie, Masahiro
Tetrahedron, 1998 , vol. 54, # 24 p. 6627 - 6638
反应条件
1: aq. NH3, H2S / methanol 2: sulfur / 150 °C 3: (i) Br2, CHCl3, (ii) aq. NaOH View Scheme
参考文献
Asinger,F. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 639, p. 133 - 146
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; dibenzoyl peroxide in tetrachloromethane 1.5 h; Heating; Product distribution;
参考文献
Krieg, Benno; Mittner, Juergen
Liebigs Annalen der Chemie, 1981 , # 4 p. 623 - 632
反应条件
1: sulfur / 150 °C 2: (i) Br2, CHCl3, (ii) aq. NaOH View Scheme
参考文献
Asinger,F. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 639, p. 133 - 146
反应条件
styrene; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube;
参考文献
Sakamoto, Takao; Nagata, Hideo; Kondo, Yoshinori; Shiraiwa, Masafumi; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 2 p. 823 - 828
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
反应条件
triethylamine; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sakamoto, Takao; Nagata, Hideo; Kondo, Yoshinori; Shiraiwa, Masafumi; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 2 p. 823 - 828
