2-氯亚甲基-丙二酸 二乙酯合成路线 （共 11 条）
反应条件
thionyl chloride; N,N-dimethyl-formamide in toluene Heating;
参考文献
Egri, Gabriella; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1997 , vol. 8, # 4 p. 547 - 557
反应条件
toluene-4-sulfonic acid
参考文献
Liard,J.-L. et al.
Bulletin de la Societe Chimique de France, 1973 , p. 3006 - 3009
反应条件
phosphorus pentachloride; trichlorophosphate
参考文献
Friedrich,K.; Thieme,H.K.
Chemische Berichte, 1970 , vol. 103, p. 1982 - 1991
反应条件
1: 2.) triethylamine / 1.) CH2Cl2, ether, -78 deg C, 5 h, 2.) CH2Cl2, ether, -78 deg C, 2 h 2: 35 percent / CH2Cl2 / 120 h View Scheme
参考文献
Nakano, Yoshihiko; Ilamaguchi, Masashi; Nagai, Toshikazu
Journal of Chemical Research, Miniprint, 1991 , # 7 p. 1701 - 1757
反应条件
sodium hydride 0.5 h;
参考文献
Egri, Gabriella; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1997 , vol. 8, # 4 p. 547 - 557
反应条件
pyridine 0.25 h; Ambient temperature;
参考文献
Egri, Gabriella; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1997 , vol. 8, # 4 p. 547 - 557
反应条件
aluminium trichloride in 1,2-dichloro-ethane
参考文献
Ertel,W.; Friedrich,K.
Chemische Berichte, 1977 , vol. 110, p. 86 - 95
反应条件
aluminium trichloride in 1,2-dichloro-ethane
参考文献
Ertel,W.; Friedrich,K.
Chemische Berichte, 1977 , vol. 110, p. 86 - 95
反应条件
sodium hydride
0.5 h;
参考文献
Egri, Gabriella; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1997 , vol. 8, # 4 p. 547 - 557
反应条件
1: 96 percent / pyridine / 0.25 h / Ambient temperature
2: 90 percent / Na / 0.5 h / 50 °C
View Scheme
参考文献
Egri, Gabriella; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1997 , vol. 8, # 4 p. 547 - 557
