N-(氨基亚胺甲基)-肼甲酰胺盐酸盐(1:2)合成路线 (共 2 条)
反应条件
hydrogenchloride; sulfuric acid; nitric acid; zinc nitro-compound obtained by treatment with a mixture of HNO3 and H2SO4; redn. with Zn-powder in concd. HCl; addn. of benzaldehyde at ambient temp.; hydrolysis of semicarbazone with concd. HCl;
参考文献
Nishikawa, T.; Miyahara, S.
Rept. Res. Sci. Dept. Kyushu Univ., 1950 , vol. 1, p. 167 - 170
C.A., 1952 , p. 3950
Full Text Show Details
Gmelin Handbook: C: MVol.D1, 48.1.5, page 461 - 461
反应条件
hydrogenchloride; sodium ethanolate the intermediate 4-(4,6-dihydroxy-pyrimidyl-(2))-semicarbazide hydrochloride is decomposed with concd. HCl;
参考文献
Nishikawa, T.; Miyahara, S.
Rept. Res. Sci. Dept. Kyushu Univ., 1950 , vol. 1, p. 167 - 170
C.A., 1952 , p. 3950
Full Text Show Details
Gmelin Handbook: C: MVol.D1, 48.1.5, page 461 - 461