N-苄氧羰基-4-哌啶磺酰氯合成路线 （共 7 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol P=2585.81 Torr; 14 h;
参考文献
WO2003/103669 A1, ;
Page 44-45 ;
WO 03/103669 A1
反应条件
chlorine in dichloromethane; water T=0°C; 4 h;
参考文献
EP1403255 A1, ;
Page 90 ;
EP 1403255 A1
反应条件
in water T=0°C; 0.5 h;
参考文献
WO2003/103669 A1, ;
Page 44-45 ;
WO 03/103669 A1
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C 3: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C 4: water; chlorine / dichloromethane / 0 - 10 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C 2: water; chlorine / dichloromethane / 0 - 10 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine / dichloromethane / 0 °C 2: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C 3: water; chlorine / dichloromethane / 0 - 10 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C 3: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C 4: water; chlorine / dichloromethane / 0 - 10 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
