in acetonitrile T=30.8°C; autocatalysis; var. conc. of reagents, other solvent, temperature and var. additives; Rate constant;
参考文献
Akinyele, Elizabeth T.; Crist, Delanson F.; Hirst, Jack
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 5 p. 905 - 909
in dichloromethane dissolving of 1.1 mmol (mer-RuCl3((CH3)2SO)3) in CH2Cl2; addn. of 4 mmol imidazole; addn. of a few drops of diethyl ether after a few minutes; pptn.; filtration after 30 min;; washing with cold CH2Cl2 and diethyl ether; drying in vac. at room temperature; elem. anal.;;
参考文献
Alessio, E.; Balducci, G.; Lutman, A.; Mestroni, G.; Calligaris, M.; Attia, W. M.
Inorganica Chimica Acta, 1993 , vol. 203, p. 205 - 218