4,7-双(5-溴-2-噻吩基)-2,1,3-苯并噻二唑合成路线 （共 5 条）
参考文献
Zhao, Xiaoyong; Piliego, Claudia; Kim, Bongsoo; Poulsen, Daniel A.; Ma, Biwu; Unruh, David A.; Frechet, Jean M. J.
Chemistry of Materials, 2010 , vol. 22, # 7 p. 2325 - 2332
反应条件
1: 81 percent / aq. Na2CO3 / Pd(PPh3)4 / benzene; ethanol / 15 h / 85 °C 2: 73 percent / NBS / CHCl3 / 48 h / 20 °C View Scheme
参考文献
Huang, Fei; Hou, Lintao; Shen, Huilin; Jiang, Jiaxing; Wang, Feng; Zhen, Hongyu; Cao, Yong
Journal of Materials Chemistry, 2005 , vol. 15, # 25 p. 2499 - 2507
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=20°C; 0.25 h;
参考文献
Li, Yilin; Scudiero, Louis; Ren, Tianhui; Dong, Wen-Ji
Journal of Photochemistry and Photobiology A: Chemistry, 2012 , vol. 231, # 1 p. 51 - 59
反应条件
1: hydrogen bromide; bromine 2: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran 3: N-bromosuccinmide; acetic acid / chloroform View Scheme
参考文献
Kim, Gyoungsik; Yeom, Hye Rim; Cho, Shinuk; Seo, Jung Hwa; Kim, Jin Young; Yang, Changduk
Macromolecules, 2012 , vol. 45, # 4 p. 1847 - 1857
反应条件
1: thionyl chloride; triethylamine / dichloromethane / Reflux 2: hydrogen bromide; bromine / Reflux 3: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / Reflux 4: N-bromosuccinmide / N,N-dimethyl-formamide / 20 °C View Scheme
参考文献
Zeng, Shaohang; Yin, Lunxiang; Jiang, Xueying; Li, Yanqin; Li, Kechang
Dyes and Pigments, 2012 , vol. 95, # 2 p. 229 - 235
