3-(4-甲氧苯基)-3-氧代丙酸乙酯合成路线 （共 58 条）
反应条件
1: 98 percent / SOCl2, pyridine / 2 h / 0 °C 2: 15 percent / toluene / 12 h / Heating View Scheme
参考文献
Lohray; Jayachandran; Bhushan; Nandanan; Ravindranathan
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5983 - 5985
反应条件
potassium tert-butylate in diethyl ether T=0 - 20°C; 10.5 h;
参考文献
Song, Dong-Po; Shi, Xin-Cui; Wang, Yong-Xia; Yang, Ji-Xing; Li, Yue-Sheng
Organometallics, 2012 , vol. 31, # 3 p. 966 - 975
反应条件
sodium Reinigung ueber das Kupfersalz;
参考文献
Menozzi, Giulia; Merello, Luisa; Fossa, Paola; Mosti, Luisa; Piana, Antonietta; Mattioli, Francesca
Farmaco, 2003 , vol. 58, # 9 p. 795 - 808
参考文献
Cabildo, Pilar; Claramunt, Rosa M.; Elguero, Jose; Foces-Foces, Concepcion; Llamas-Saiz, Antonio L.; Cano, Felix H.
Bulletin des Societes Chimiques Belges, 1993 , vol. 102, # 11/12 p. 735 - 748
反应条件
1: 1.) sodium wire / 1) ether; 2) ether, reflux, 5 h 2: sodium acetate / aq. ethanol / 6 h / Heating View Scheme
参考文献
Tranquillini
Farmaco, 1992 , vol. 47, # 10 p. 1323 - 1333
反应条件
sodium hydride in ethylene glycol dimethyl ether; paraffin 4 h; Heating;
参考文献
Specht, Donald P.; Martic, Peter A.; Farid, Samir; ++
Tetrahedron, 1982 , vol. 38, # 9 p. 1203 - 1211
反应条件
zinc; diisobutylaluminium hydride; palladium 1.) DME; 2.) DME, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Sato, Toshio; Itoh, Toshiyuki; Fujisawa, Tamotsu
Chemistry Letters, 1982 , p. 1559 - 1560
反应条件
in toluene 12 h; Heating;
参考文献
Lohray; Jayachandran; Bhushan; Nandanan; Ravindranathan
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5983 - 5985
反应条件
1: 88 percent / oxalyl chloride / benzene; dimethylformamide / Ambient temperature 2: 1.) sodium wire / 1) ether; 2) ether, reflux, 5 h 3: sodium acetate / aq. ethanol / 6 h / Heating View Scheme
参考文献
Schoonjans
Chem. Zentralbl., 1897 , vol. 68, # II p. 616
反应条件
triethylamine; magnesium chloride multistep reaction; other acid chlorides, other solvent;
参考文献
Clay; Collom; Karrick; Wemple
Synthesis, 1993 , # 3 p. 290 - 292
