N-Boc-3-羟基-D-缬氨酸合成路线 （共 3 条）
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in phosphate buffer; acetonitrile T=35°C;
参考文献
Inoue, Masayuki; Shinohara, Naoki; Tanabe, Shintaro; Takahashi, Tomoaki; Okura, Ken; Itoh, Hiroaki; Mizoguchi, Yuki; Iida, Maiko; Lee, Nayoung; Matsuoka, Shigeru
Nature Chemistry, 2010 , vol. 2, # 4 p. 280 - 285
反应条件
trifluoroacetic acid in dichloromethane
参考文献
Inoue, Masayuki; Shinohara, Naoki; Tanabe, Shintaro; Takahashi, Tomoaki; Okura, Ken; Itoh, Hiroaki; Mizoguchi, Yuki; Iida, Maiko; Lee, Nayoung; Matsuoka, Shigeru
Nature Chemistry, 2010 , vol. 2, # 4 p. 280 - 285
反应条件
1: (R)-N-Boc-2-amino-3-hydroxy-3-methylbutanoic acid With trifluoroacetic acid in dichloromethane
2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione With sodium hydrogencarbonate in water; acetone
参考文献
Valorisation HSJ, Societe en Commandite
Patent: US2009/48161 A1, 2009 ;
Location in patent: Page/Page column 40 ;
