Jones, Amanda C.; Sanders, Aaron W.; Sikorski, William H.; Jansen, Kristin L.; Reich, Hans J.
Journal of the American Chemical Society, 2008 , vol. 130, # 19 p. 6060 - 6061
in tetrahydrofuran; diethyl ether
under dry nitrogen; a THF solution of TsiLi was added with stirring (0,5 h) to a 1/3 THF/Et2O mixture of tin compound at room temperature; 1 h reflux;; solvent removed; extraction (CH2Cl2); extract was filtered and evaporated; residue was recrystd. (MeOH); elem. anal.;
参考文献
Dhaher, Saadi M.; Eaborn, Colin; Smith, J. David
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 33 - 44
