反应条件
in tetrahydrofuran
addn. of B(OMe)3 to soln. of LiC(SiMe3)3 (stirring, (1)H- and (11)B-NMR monitoring), pptn.; removal of solvent, washing (water), shaking (light petroleum b.p. 60-80°C), refluxing of solid (THF/water 4:1), evapn. of solvent, sublimation (70°C, 0.1 Torr), recrystn. (pentane); elem anal.;
参考文献
Al-Juaid, Salih S.; Eaborn, Colin; El-Kheli, Mohamed N. A.; Hitchcock, Peter R.; Lickiss, Paul D.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 447 - 452
