addn. of BBr3 to solid boroxine at 30 Torr and heating of react. vessel to 100°C; more volatile react. products (B2H6 and B2H5Br) removed by cooling of react. mixt. to -78°C, residue is HBBr2/BBr3 mixt.;
参考文献
Journal of Physical Chemistry, , # 69 p. 2461 - 2462
Wason, S. K.; Porter, R. F.
Journal of Physical Chemistry, 1965 , # 69 p. 2461 - 2462
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Gmelin Handbook: B: B-Verb.9, 1.2.3.3, page 31 - 31