hydrogen; palladium on activated charcoal in methanol T=20°C; P=760 Torr;
参考文献
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415
1: 1) butyllithium, di-isopropylamine / 1) THF, 0 deg C, 1 h 2) THF, -70 deg C, 3 h 2: 70 percent / chromic anhydride / acetone / 3 h / Ambient temperature 3: hydrogen / Pd-C / methanol / 20 °C / 760 Torr 4: 100 percent View Scheme
参考文献
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415
1: 1) butyllithium, di-isopropylamine / 1) THF, 0 deg C, 1 h 2) THF, -70 deg C, 3 h 2: 70 percent / chromic anhydride / acetone / 3 h / Ambient temperature 3: hydrogen / Pd-C / methanol / 20 °C / 760 Torr 4: 100 percent View Scheme
参考文献
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415