反应条件
1: thionyl chloride / toluene
2: 1,3-bis-(1-adamantyl)imidazolinium tetrafluoroborate; palladium diacetate; n-ethyl morpholine / para-xylene / 3 h / 115 - 120 °C / |Inert atmosphere
3: dimethylsulfide; boron trifluoride diethyl etherate / dichloromethane / 20 h / |Inert atmosphere
View Scheme
参考文献
Acerson, Mark J.; Fabick, Kimberly M.; Wong, Yong; Blake, Crystal; Lephart, Edwin D.; Andrus, Merritt B.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 10 p. 2941 - 2944
