3,4-二氯-3-环丁烯-1,2-二酮合成路线 （共 26 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rubin, Yves; Knobler, Carolyn B.; Diederich, Francois
Journal of the American Chemical Society, 1990 , vol. 112, # 4 p. 1607 - 1617
反应条件
aluminium trichloride
参考文献
Maahs,G.; Hegenberg,P.
Angewandte Chemie, 1966 , vol. 78, p. 927 - 931
Full Text Show Details
Green,B.R.; Neuse,E.W.
Synthesis, 1974 , p. 46 - 47
反应条件
T=700°C; Ring cleavage; P=0.00075 Torr;
参考文献
Bock, Hans; Ried, Walter; Stein, Udo
Chemische Berichte, 1981 , vol. 114, # 2 p. 673 - 683
反应条件
in gaseous matrix
T=-263.2°C; Irradiationdifferent reaction times; Mechanism;
参考文献
Mincu; Hillebrand; Allouche; Cossu; Verlaque; Aycard; Pourcin
Journal of Physical Chemistry, 1996 , vol. 100, # 40 p. 16045 - 16052
反应条件
N,N-dimethyl-formamide in dichloromethane
1) 2 h, room temp.; 30 min, reflux;
参考文献
Schmidt, Arthur H.; Plaul, Wolfgang; Aimene, Amokrane; Hotz, Monika; Hoch, Monika
Liebigs Annalen der Chemie, 1985 , # 5 p. 1021 - 1035
反应条件
in benzene
0.5 h; Heating;
参考文献
Schmidt, Arthur H.; Plaul, Wolfgang; Aimene, Amokrane; Hotz, Monika; Hoch, Monika
Liebigs Annalen der Chemie, 1985 , # 5 p. 1021 - 1035
反应条件
triethylamine in benzene
2 h; Heating;
参考文献
Fu, Nanyan; Allen, Annette D.; Kobayashi, Shinjiro; Tidwell, Thomas T.; Vukovic, Sinisa; Matsuoka, Takeshi; Mishima, Masaaki
Journal of Organic Chemistry, 2008 , vol. 73, # 5 p. 1768 - 1773
反应条件
aluminium trichloride in dichloromethane
Friedel-Crafts reaction; Heating;
参考文献
Liu, Zong-Ying; Wang, Yue-Ming; Han, Yan-Xing; Liu, Ling; Jin, Jie; Yi, Hong; Li, Zhuo-Rong; Jiang, Jian-Dong; Boykin, David W.
European Journal of Medicinal Chemistry, 2013 , vol. 65, p. 187 - 194
反应条件
N,N-dimethyl-formamide in dichloromethane
1) 2 h, room temp.; 30 min, reflux;
参考文献
Schmidt, Arthur H.; Plaul, Wolfgang; Aimene, Amokrane; Hotz, Monika; Hoch, Monika
Liebigs Annalen der Chemie, 1985 , # 5 p. 1021 - 1035
反应条件
N,N-dimethyl-formamide in dichloromethane
1) 2 h, room temp.; 30 min, reflux;
参考文献
Schmidt, Arthur H.; Plaul, Wolfgang; Aimene, Amokrane; Hotz, Monika; Hoch, Monika
Liebigs Annalen der Chemie, 1985 , # 5 p. 1021 - 1035
