2-甲基-3-呋喃羧酸乙酯合成路线 (共 24 条)
反应条件
pyridine in water T=20°C; 24 h;
参考文献
Nazef, Naim; Davies, Robert D. M.; Greaney, Michael F.
Organic Letters, 2012 , vol. 14, # 14 p. 3720 - 3723
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
Kretchmer; Richard Allan; Laitar; Robert Anton
Patent: US4025537 A1, 1977 ;
反应条件
toluene-4-sulfonic acid in benzene T=90°C; 4 h;
参考文献
Corey, E. J.; Ghosh, Arun K.
Chemistry Letters, 1987 , p. 223 - 226
参考文献
Gilman et al.
Recueil des Travaux Chimiques des Pays-Bas, 1932 , vol. 51, p. 407,409
Full Text Show Details
Gilman; Burtner
Iowa State College Journal of Science, 1931 , vol. 5, p. 189,191
反应条件
1: cobalt(II) chloride / acetonitrile / 3 h / 85 °C / |Inert atmosphere; |Schlenk technique 2: trifluorormethanesulfonic acid / acetonitrile / 1 h / 85 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Antonioletti, Roberto; Bonadies, Francesco; Scettri, Arrigo
Gazzetta Chimica Italiana, 1988 , vol. 118, # 1 p. 73 - 74
反应条件
in benzene T=80°C; 4 h; Yields of byproduct given;
参考文献
Pevzner, L. M.; Ignat'ev, V. M.; Ionin, B. I.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.1 p. 797 - 803,658 - 662
反应条件
1: NaIO4 / methanol; H2O / 24 h / Ambient temperature 2: pyridine / CCl4 / 2 h / Heating View Scheme
参考文献
Lee Yong Rok, R.; Kim, Nam Suk; Kim, Byung So
Tetrahedron Letters, 1997 , vol. 38, # 32 p. 5671 - 5674
反应条件
1: With ammonium hydroxide in water 2: With hydrogenchloride in diethyl ether; water
参考文献
Skaddan, Marc B.
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 2 p. 73 - 77
反应条件
in toluene Heating; Yield given;
参考文献
Antonioletti, Roberto; Bonadies, Francesco; Scettri, Arrigo
Gazzetta Chimica Italiana, 1988 , vol. 118, # 1 p. 73 - 74
反应条件
T=190°C; 15 h; Yield given. Yields of byproduct given;
参考文献
Jaworski, Tadeusz; Mizerski, Tadeusz
Polish Journal of Chemistry, 1981 , vol. 55, # 2 p. 317 - 320