2-甲基-3-呋喃羧酸乙酯合成路线 （共 24 条）
反应条件
1: LiAlH4
2: 92 percent / Et3N / diethyl ether / 10 h / Ambient temperature
3: 635 °C / 0 Torr
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参考文献
Trahanovsky,W.S.; Cassidy,T.J.; Woods,T.L.
Journal of the American Chemical Society, 1981 , vol. 103, p. 6691
反应条件
1: 52 percent / LiAlH4
2: 1.) Br2, 2.) Et3N / 1.) Et2O, -78 deg C, 1.5 h, 2.) -78 deg C -> room temperature
3: 50 percent / hydroquinone / dioxane; H2O / 1 h / Heating; phosphate buffer (pH 6.3)
View Scheme
参考文献
Nazef, Naim; Davies, Robert D. M.; Greaney, Michael F.
Organic Letters, 2012 , vol. 14, # 14 p. 3720 - 3723
反应条件
nitric acid; acetic anhydride
T=-25°C;
参考文献
Gilman; Burtner
Iowa State College Journal of Science, 1931 , vol. 5, p. 189,191
反应条件
carbon disulfide; aluminium trichloride
参考文献
Messina; Brown
Journal of the American Chemical Society, 1952 , vol. 74, p. 1087
