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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
28940-48-9
合成路线
(共 4 条)
28940-47-8
→
反应条件
28940-48-9
反应条件
1: With hydrogenchloride; SnCl2·2H2O in ethanol; water T=75°C; 1 h; 2: With sodium hydroxide in water Cooling with ice;
参考文献
Vitale, Gabriella; Corona, Paola; Loriga, Mario; Carta, Antonio; Paglietti, Giuseppe; Ibba, Cristina; Giliberti, Gabriele; Loddo, Roberta; Marongiu, Esther; La Colla, Paolo
Medicinal Chemistry, 2010 , vol. 6, # 2 p. 70 - 78
49678-08-2
对硝基肉桂醛
→
反应条件
28940-48-9
反应条件
1.1: Na2S2O5 / ethanol / 20 °C 2.1: ethanol / 4 h / Reflux 3.1: hydrogenchloride; SnCl2·2H2O / ethanol; water / 1 h / 75 °C 3.2: Cooling with ice View Scheme
参考文献
Vitale, Gabriella; Corona, Paola; Loriga, Mario; Carta, Antonio; Paglietti, Giuseppe; Ibba, Cristina; Giliberti, Gabriele; Loddo, Roberta; Marongiu, Esther; La Colla, Paolo
Medicinal Chemistry, 2010 , vol. 6, # 2 p. 70 - 78
1238855-02-1
→
反应条件
28940-48-9
反应条件
1.1: ethanol / 4 h / Reflux 2.1: hydrogenchloride; SnCl2·2H2O / ethanol; water / 1 h / 75 °C 2.2: Cooling with ice View Scheme
参考文献
Vitale, Gabriella; Corona, Paola; Loriga, Mario; Carta, Antonio; Paglietti, Giuseppe; Ibba, Cristina; Giliberti, Gabriele; Loddo, Roberta; Marongiu, Esther; La Colla, Paolo
Medicinal Chemistry, 2010 , vol. 6, # 2 p. 70 - 78
95-54-5
1,2-苯二胺
→
反应条件
28940-48-9
反应条件
1.1: ethanol / 4 h / Reflux 2.1: hydrogenchloride; SnCl2·2H2O / ethanol; water / 1 h / 75 °C 2.2: Cooling with ice View Scheme
参考文献
Vitale, Gabriella; Corona, Paola; Loriga, Mario; Carta, Antonio; Paglietti, Giuseppe; Ibba, Cristina; Giliberti, Gabriele; Loddo, Roberta; Marongiu, Esther; La Colla, Paolo
Medicinal Chemistry, 2010 , vol. 6, # 2 p. 70 - 78