1,3,5,7,2,4,6,8-四硫杂四氮杂环辛四烯合成路线 (共 142 条)
参考文献
Gmelin Handbook: Hg: MVol.B1, 9, page 240 - 261
反应条件
in tetrachloromethane
introduction of dry HBr (react. cotrolled by addn. of CO2) into soln. of S4N4 in CCl4; pptn.;; filtration; washing; drying (clay/desiccator - vac.);
参考文献
Gmelin Handbook: S: MVol.B3, 160, page 1868 - 1870
反应条件
in hexane
not isolated;
参考文献
Pritchina, Elena A.; Terpilovskaya, Daria S.; Tsentalovich, Yuri P.; Platz, Matthew S.; Gritsan, Nina P.
Inorganic Chemistry, 2012 , vol. 51, # 8 p. 4747 - 4755
参考文献
Ruff, O.; Geisel, E.
Ber., 1904 , vol. 37, p. 1573 - 1595
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 7, page 1545 - 1547
参考文献
Ruff, O.; Geisel, E.
Ber., 1904 , vol. 37, p. 1573 - 1595
反应条件
silver in neat (no solvent)
参考文献
Woollins, J. Derek
Polyhedron, 1987 , vol. 6, p. 939 - 942
反应条件
in neat (no solvent, gas phase)
by pyrolysis of S4N4 over glass (275°C) or silver wool (according to Smith, R. D., J. Chem. Soc., Dalton Trans. 1979, 478-481);
参考文献
Lau, W. M.; Westwood, N. P. C.; Palmer, M. H.
Journal of the American Chemical Society, 1986 , vol. 108, # 12 p. 3229 - 3237
反应条件
carbon dioxide in water
CO2 satd. soln. (acidic), 8 days shaking, 0°C;;
参考文献
Jeroch, W.
Diss. Berlin 1906, S. 25
反应条件
in not given
in acidic soln.;
参考文献
Gmelin Handbook: S: MVol.B2, 11, page 992 - 1010
反应条件
water; hydroxide in water
byproducts: H(1+); hydrolysis;;
参考文献
Gmelin Handbook: S: MVol.B3, 7, page 1545 - 1547