dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran; water
T=60°C; Suzuki-Miyaura cross-coupling; 21 h;
参考文献
Antelo Miguez, Jose M.; Adrio, Luis Angel; Sousa-Pedrares, Antonio; Vila, Jose M.; Hii, King Kuok
Journal of Organic Chemistry, 2007 , vol. 72, # 20 p. 7771 - 7774
1: K3PO4 / Pd(OAc)2 / dimethylformamide; H2O / 3 h / 20 °C
2: (2',6'-dimethoxybiphenyl-2-yl)dicyclohexylphosphine / Pd3(OAc)6 / tetrahydrofuran; H2O / 21 h / 60 °C
View Scheme
参考文献
Antelo Miguez, Jose M.; Adrio, Luis Angel; Sousa-Pedrares, Antonio; Vila, Jose M.; Hii, King Kuok
Journal of Organic Chemistry, 2007 , vol. 72, # 20 p. 7771 - 7774
Jo, Hyunjong; Kim, Chul-Bae; Ryoo, Tae-Yong; Ahn, Bo-Kyoung; Park, Kwangyong
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 12 p. 3749 - 3754