2-羟基-5-碘-3-甲基吡啶合成路线 (共 2 条)
反应条件
1: With sulfuric acid; sodium nitrite T=60°C; 0.25 h; 2: With boric acid in water T=0 - 100°C;
参考文献
Lan, Tao; McLaughlin, Larry W.
Journal of the American Chemical Society, 2000 , vol. 122, # 27 p. 6512 - 6513
反应条件
1.1: 73 percent / periodic acid dihydrate; iodine; sulfuric acid / acetic acid; H2O / 4 h / 80 °C 2.1: conc. sulfuric acid; sodium nitrite / 0.25 h / 60 °C 2.2: 75 percent / boric acid / 100 °C View Scheme
参考文献
Lan, Tao; McLaughlin, Larry W.
Bioorganic Chemistry, 2001 , vol. 29, # 4 p. 198 - 210