N-乙酰-DL-苯丙氨酸合成路线 （共 69 条）
反应条件
hydrogenchloride in water T=95 - 100°C; 6 h; Overall yield = 66.6 percent;
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
ammonium hydroxide; anhydrous cobalt diacetate T=37°C; 24 h; aminoacylase from Aspegillus; Yield given. Yields of byproduct given;
参考文献
Kitahara, Toshio; Asai, Soichiro
Agricultural and Biological Chemistry, 1983 , vol. 47, # 5 p. 991 - 996
反应条件
dicyclohexyl-carbodiimide
参考文献
Lyubeznova, M. R.; Karpeiskaya, E. I.; Klabunovskii, E. I.; Koreshkov, Yu. D.; Lutsenko, A. I.; Lubuzh, E. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.1 p. 731 - 737
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 823 - 828
反应条件
(i) ClCO2Et, Et3N, (ii) /BRN= 1735708/; Multistep reaction;
参考文献
Gillis; Kadunce
The Journal of organic chemistry, 1967 , vol. 32, # 1 p. 91 - 94
反应条件
2: 35 percent Chromat. / 0 °C / Irradiation; filter: solution of sodium hydrogen phthalate-NaNO2
View Scheme
参考文献
Chow, Yuan L.; Polo, Joel S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 727 - 734
反应条件
graphite electrode in methanol
T=15°C; Electrochemical reaction; Product distribution; Further Variations:Reagents;
参考文献
Ungureanu, Eleonora Mihaela; Stanciu, Gabriela; Rosca, Sorin Ioan
Revue Roumaine de Chimie, 2000 , vol. 45, # 9 p. 869 - 875
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=0°C; 1 h;
参考文献
Kim, Yongju; Kim, Jonghoon; Park, Seung Bum
Organic Letters, 2009 , vol. 11, # 1 p. 17 - 20
反应条件
dicyclohexyl-carbodiimide in dichloromethane
168 h; Ambient temperature;
参考文献
Andersen, Kenneth K.; Gloster, Daniel F.; Bray, Diana D.; Shoja, Massud; Kjaer, Anders
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 2 p. 317 - 324
反应条件
2: 3 percent Chromat. / 0 °C / Irradiation; filter: solution of sodium hydrogen phthalate-NaNO2
View Scheme
参考文献
Chow, Yuan L.; Polo, Joel S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 727 - 734
