2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
1: 80 percent / PCl5 / 130 °C
2: 75 percent
View Scheme
参考文献
Fischer, Ulrich; Haegele, Gerhard
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 9 p. 1152 - 1156
反应条件
Aliquatreg; 336; sodium carbonate in acetonitrile
T=80°C; 2 h;
参考文献
Atanassova, I.A.; Petrov, J.S.; Ognjanova, V.H.; Mollov, N.M.
Synthetic Communications, 1990 , vol. 20, # 14 p. 2083 - 2090
反应条件
phosphorus pentachloride
T=130°C;
参考文献
Fischer, Ulrich; Haegele, Gerhard
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 9 p. 1152 - 1156
参考文献
du Pont de Nemours and Co.
Patent: US2351247 , 1941 ;
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2390629 , 1943 ;
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent)
T=20 - 25°C; 12 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
in hexane
0.5 h; Ambient temperature;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
in hexane
0.5 h; Ambient temperature;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
in tetrahydrofuran; water
T=20°C; 1 h; Inert atmosphere;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
参考文献
Houben; Fischer
Chemische Berichte, 1931 , vol. 64, p. 240,247, 2636, 2642
参考文献
Houben; Fischer
Chemische Berichte, 1931 , vol. 64, p. 240,247, 2636, 2642
