2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
4-nitro-phenol; N,N,N',N'',N''-pentamethyldiethylenetriamine in acetonitrile
T=20 - 25°C; 36 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
in dichloromethane
T=25°C; Rate constant;
参考文献
Druzian, Janice; Zucco, Cesar; Rezende, Marcos Caroli; Nome, Faruk
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4767 - 4771
反应条件
in hexane
0.5 h; Ambient temperature;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
sodium hydroxide in dimethyl sulfoxide
T=80°C; 2 h;
参考文献
Atanassova, I.A.; Petrov, J.S.; Ognjanova, V.H.; Mollov, N.M.
Synthetic Communications, 1990 , vol. 20, # 14 p. 2083 - 2090
反应条件
potassium acetate
T=150°C; unter Ausschluss von Feuchtigkeit;
参考文献
Houben; Fischer
Chemische Berichte, 1931 , vol. 64, p. 2636,2639
反应条件
triethylamine in acetonitrile
5 h; Heating;
参考文献
Rebelo, Ricardo Andrade; Rezende, Marcos Caroli; Nome, Faruk; Zucco, Cesar
Synthetic Communications, 1987 , vol. 17, # 14 p. 1741 - 1748
反应条件
hydrogen fluoride; silver fluoride
参考文献
Simons; Herman
Journal of the American Chemical Society, 1943 , vol. 65, p. 2064
反应条件
p-cresol; N,N,N',N'',N''-pentamethyldiethylenetriamine in acetonitrile
T=20 - 25°C; 6 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
1: PCl5 / 220 °C
2: anhydrous HF / 145 - 155 °C / 14710.2 Torr
3: AgF / 180 °C
View Scheme
参考文献
Simons; Herman
Journal of the American Chemical Society, 1943 , vol. 65, p. 2064
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent)
T=20 - 25°C; 15 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
