2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent) T=20 - 25°C; 2 h;
参考文献
Tetrahedron, , vol. 68, # 44 p. 9068 - 9075
反应条件
in acetonitrile T=25°C; Rate constant;
参考文献
Druzian, Janice; Zucco, Cesar; Rezende, Marcos Caroli; Nome, Faruk
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4767 - 4771
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine; aniline in acetonitrile T=20 - 25°C; 0.5 h;
参考文献
Tetrahedron, , vol. 68, # 44 p. 9068 - 9075
反应条件
triethylamine T=25°C; 4 h;
参考文献
Hess, Sonia Corina; Nome, Faruk; Zucco, Cesar; Rezende, Marcos Caroli
Synthetic Communications, 1989 , vol. 19, # 17 p. 3037 - 3046
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent) T=20 - 25°C; 12 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
ethylamine T=25°C; var. concn. of ethylamine; Rate constant;
参考文献
Uieara, Marina; Zucco, Cesar; Zanette, Dino; Rezende, Marcos C.; Nome, Faruk
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 175 - 180
反应条件
N,N,N',N'',N''-pentamethyldiethylenetriamine in neat (no solvent) T=20 - 25°C; 12 h;
参考文献
Ram, Ram N.; Soni, Vineet Kumar; Gupta, Dharmendra Kumar
Tetrahedron, 2012 , vol. 68, # 44 p. 9068 - 9075
反应条件
ethylamine T=25°C; Rate constant;
参考文献
Uieara, Marina; Zucco, Cesar; Zanette, Dino; Rezende, Marcos C.; Nome, Faruk
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 175 - 180
反应条件
NaOD; water-d2 T=-78°C;
参考文献
Boyer et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 770
反应条件
1: cathecolborane / (5S)-2-(n-butyl)-4,4-diphenyl-3,1,2-oxazaborabicyclo<3.3.0>octane / toluene / 12 h / -78 °C 2: NaCNBH3, AIBN, Bu3SnCl / ethanol / Heating 3: 2M NaOH / diethyl ether / Ambient temperature View Scheme
参考文献
Corey, E. J.; Helal, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5227 - 5230
