2,2,2-三氯苯乙酮合成路线 （共 148 条）
反应条件
T=25°C; 1 h; Irradiation; Product distributionMechanism;
参考文献
Izawa, Yasuji; Tomioka, Hideo; Natsume, Masashi; Beppu, Shinji; Tsujii, Hideo
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4835 - 4838
反应条件
T=25°C; 1 h; Irradiation; Product distributionMechanism;
参考文献
Izawa, Yasuji; Tomioka, Hideo; Natsume, Masashi; Beppu, Shinji; Tsujii, Hideo
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4835 - 4838
反应条件
zinc in N,N-dimethyl-formamide 0.333333 h; Title compound not separated from byproducts;
参考文献
Shchepin, V. V.; Russkikh, N. Yu.; Rybakova, M. N.; Lapkin, I. I.; Petukhova, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 844 - 847
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 934 - 937
反应条件
sodium dichromate; sulfuric acid in acetic acid
0.166667 h; Ambient temperature;
参考文献
Gallina, Carlo; Giordano, Cesare
Synthesis, 1989 , # 6 p. 466 - 468
反应条件
trichloroisocyanuric acid; boron trifluoride diethyl etherate in acetic acid
5 h; Heating;
参考文献
Hiegel, Gene A.; Peyton, Kim B.
Synthetic Communications, 1985 , vol. 15, # 5 p. 385 - 392
反应条件
1: bromobenzene With magnesium; lithium chloride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
2: chloral in tetrahydrofuran
T=0°C; 0.5 h; Inert atmosphere;
3: With tert-butylhypochlorite in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
反应条件
aluminium trichloride
Substitution; Friedel-Crafts reaction;
参考文献
Matsuda, Tomoko; Harada, Tadao; Nakajima, Nobuyoshi; Itoh, Toshiyuki; Nakamura, Kaoru
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 157 - 163
反应条件
1: T=0°C; 0.5 h;
2: With tert-butylhypochlorite; iodine
T=20°C; 1 h; Reagent/catalyst;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
反应条件
1: T=0°C; 0.5 h;
2: With tert-butylhypochlorite; iodine
T=20°C; 4 h;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
反应条件
1: T=0°C; 0.5 h;
2: With tert-butylhypochlorite; potassium iodide
T=20°C; 4 h; Reagent/catalyst;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
